| Day | Time | Description | |
|
|
|||
|
|
|||
| 1 | Forenoon | 09:30-11:00 | Lecture: Fundamentals of NMR, Signal generation, Description of pulse and Fourier transform NMR |
| Afternoon | 14:00-15:30 |
Video: Sample preparation, understanding the parts of the NMR spectrometer and magnet. Video: Steps required for measuring 1D spectra, Shimming, locking, description of acquisition parameter. Video: Measurement of 1D NMR spectra (1H and 13C), Processing of NMR spectra, Integration, plotting, presentation of spectra, automation |
|
|
|
|||
| 2 | Forenoon | 09:30-11:00 | Lecture: NMR spectral analysis of 1D and 2D NMR |
| Afternoon | 14:00-15:30 |
Video: Steps required for measuring 2D NMR (COSY, HSQC), parameter set up, acquisition setup etc. Video: Measuring different 2D NMR Video: Processing and Analysis of measured 2D spectra, plotting and printing Lecture: Principle & applications of essential techniques in Chemistry laboratory (TGA, DSC, FT-IR, CD, CV etc.) Video: Acquisition and Analysis of these techniques |
|
|
|
|||
| 3 | Forenoon | 09:30-10:30 | Lecture: Fundamentals of TEM |
| 10:30-11:00 | Tea break | ||
| 11:00-12:30 | Video: sample preparation, sample loading, data acquiring and analysis | ||
| Afternoon | 14:00-15:00 | Lecture: Fundamentals of SEM | |
| 15:00-15:30 | Tea break | ||
| 15:30-18:00 | Video: sample preparation, sample loading, data acquiring and analysis | ||
|
|
|||
|
|
|||
| 4 | Forenoon | 09:30-11:00 | Lecture: Crystallographic symmetry and crystal systems, fundamentals of X-Ray diffraction |
| 11:30-13:00 |
Video: Understanding the parts of the X-ray diffractometer. Video: Mounting the crystal, evaluation of quality of crystal, unit cell data collection, full data collection Video: Working up raw data for modeling |
||
| Afternoon | 14:00-15:00 | Lecture: Modeling of crystal structure (without disorder) and CIF file preparation | |
| 15:15-17:15 | Lecture: Modeling of crystal structure (with disorder) and CIF file preparation | ||
|
|
|||
|
|
|||
| 5 | Forenoon | 09:30-11:30 |
Lecture: Principle and Type of Mass Spectrometry. Lecture: Fragmentation and Spectral Analysis including EI and CI ionization. Video: Components of GC-MS including column oven and mass analyzer. Video: Sample preparation, creating methods, inject through GC column and direct injection to MS without using GC column. |
| 12:00-13:00 | Lecture: Principle of ESI and MALDI including APCI and APPI | ||
| Afternoon | 14:00-18:00 |
Video: Components of MS including HR Q-Exactive Orbitrap, TOF, MALDI and Ion-Trap. Video: Sample preparation, creating methods, understanding the auto sampler and cleaning methods. Inject samples with and without column. Video: Analysis of the spectra using the software. |
|
